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The NMR spectrum has a one proton singlet at 5.93 ppm, not coupled to other protons and assigned as H11, the only proton on a carbon of the 6-membered ring
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10.1186/s10194-016-0631-z [DOI] [PMC free article] [PubMed] [Google Scholar] 57.Yin Z, Fang Y, Ren L, Wang X, Zhang A, Lin J, et al
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